Samsung RT34M Uživatelský manuál stáhnout pdf (Strana 74)

Dushyant Patel LC-MS/MS Method

S.K.P.C.P.E.R., Kherva 62 M .Pharm. Thesis

TABLE NO: 4.23

MAIN STOCK SOLUTION STABILITY OF LEV (93 hrs at room temp.)

Sr. No.

LEV(1.50 µg/ml)

Comp. sample area Stability sample area

1 6065366 6036516

2 6062324 6008907

3 6155877 5863199

4 5971748 5993892

5 5962427 5891232

6 6044741 6001840

n 6 6

Mean 6043747 5965931

SD 70970 70759

% CV 1.17 1.19

% Mean Change -1.29

TABLE NO: 4.24

MAIN STOCK SOLUTION STABILITY OF GBP (93 hrs at 2-8˚C)

Sr. No.

GBP(12.00 µg/ml)

Comp. sample area Stability sample area

1 37965530 39114837

2 37885805 40092928

3 38242777 40095247

4 38073735 40644570

5 37874277 40215347

6 38241913 40394861

n 6 6

Mean 38047340 40092965

SD 167026 522901

% CV 0.44 1.30

% Mean Change 5.38

TABLE NO: 4.25

MAIN STOCK SOLUTION STABILITY OF LEV (93 hrs at 2-8˚C)

Sr. No.

LEV(1.50 µg/ml)

Comp. sample area Stability sample area

1 6065366 5829432

2 6062324 5914353

3 6155877 5875641

4 5971748 5931620

5 5962427 5958053

6 6044741 5901846

n 6 6

Mean 6043747 5901824

SD 70970 45017

% CV 1.17 0.76

% Mean Change -2.35

4.3.10.2 Bench top stability of GBP (at room temp. for 20 hrs):

¾ LQC and HQC samples were spiked in human plasma and were kept at room

temperature for 20 hrs and were processed and analyzed along with previously bulk

1 2 ... 69 70 71 72 73 74 75 76 77 78 79 ... 92 93

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