Samsung RT34M Uživatelský manuál stáhnout pdf (Strana 24)

Dushyant Patel Review of Literature

S.K.P.C.P.E.R., Kherva 12 M .Pharm. Thesis

16. Simultaneous isocratic HPLC

determination of vigabatrin and

gabapentin in human plasma by

dansyl derivatization

17

.

HPLC Derivatization reagent: Dansyl

chloride

Column: Micro bondapak C-

18, 10 µ , 300 x 3.9 mm

MP: 50 mmol/l NaH

2

PO

4

in

40% ACN

Detection method: Fluorimetry

(EX: 318 nm, EM: 510 nm)

17. Determination of gabapentin in

serum using solid-phase extraction

and gas-liquid chromatography

18

.

GLC Extraction method: SPE on

C18 solid-phase column

Derivatization reagent:

MTBSTFA plus 1% tBDMCS

Column : HP-1

Detector: FID

IS: [(1-aminomethyl-1-

cycloheptyl) acetic acid]

18. Determination of gabapentin in

serum by capillary

electrophoresis

19

.

CE

Derivatization reagent:

fluorescamine

Detection method: UV-

fluorescence detection

19. Determination of gabapentin in

human plasma by capillary

electrophoresis with laser-induced

fluorescence detection and

acetonitrile stacking technique

20

.

CE

Derivatization reagent:

6-Carboxyfluorescein

succinimidyl ester (CFSE)

Buffer: 50 mM sodium borate

(pH 9.5)

Detection method:

Fluorimetry (EX: 488 nm, EM:

520 nm)

20. Spectrofluorimetric determination

of vigabatrin and gabapentin in

urine and dosage forms through

derivatization with fluorescamine

21

.

Spectrofluor

imetry

Derivatization reagent:

fluorescamine

Detection method:

Spectrofluorimetry

(EX: 390 nm, EM: 472 nm)

1 2 ... 19 20 21 22 23 24 25 26 27 28 29 ... 92 93

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