Samsung RT34M Uživatelský manuál stáhnout pdf (Strana 66)

Dushyant Patel LC-MS/MS Method

S.K.P.C.P.E.R., Kherva 54 M .Pharm. Thesis

TABLE NO: 4.13

SUMMARY OF CALIBRATION CURVE PARAMETERS OF GBP

Sr. No. SLOPE INTERCEPT r r

1 0.7104 -0.0004 0.9995

0.9991

2 0.7685 0.0020 0.9997 0.9994

3 0.6659 0.0033 0.9997 0.9994

4 0.6993 0.0029 0.9988 0.9976

5 0.7235 0.0029 0.9988 0.9976

TABLE NO: 4.14

BACK CALCULATED CONCENTRATION OF CALIBRATION STANDARDS FROM

CALIBRATION CURVE OF GBP

LINEARITY

Conc. (µg/ml)

Sr.

No.

CS-1 CS-2 CS-3 CS-4 CS-5 CS-6 CS-7 CS-8 CS-9

0.05 0.10 0.30 0.60 1.20 2.40 3.60 4.80 6.00

% Nominal

Deviation

0.049 0.104 0.293 0.578 1.205 2.331 3.715 4.905 6.030

-2.00 4.00 -2.33 -3.67 0.42 -2.88 3.19 2.19 0.50

% Nominal

Deviation

0.050 0.101 0.294 0.609 1.153 2.392 3.708 4.802 6.075

0.00 1.00 -2.00 1.50 -3.92 -0.33 3.00 0.04 1.25

% Nominal

Deviation

0.050 0.100 0.293 0.592 1.189 2.378 3.750 4.747 6.100

0.00 0.00 -2.33 -1.33 -0.92 -0.92 4.17 -1.10 1.67

% Nominal

Deviation

0.051 0.095 0.281 0.640 1.177 2.349 3.762 4.775 6.093

2.00 -5.00 -6.33 6.67 -1.92 -2.12 4.50 -0.52 1.55

% Nominal

Deviation

0.051 0.096 0.283 0.654 1.190 2.373 3.707 4.777 5.864

2.00 -4.00 -5.67 9.00 -0.83 -1.12 2.97 -0.48 -2.27

Mean 0.050 0.099 0.289 0.615 1.183 2.365 3.728 4.801 6.032

SD 0.001 0.003 0.006 0.029 0.017 0.022 0.023 0.055 0.088

%CV 2.00 3.03 2.08 4.72 1.44 0.93 0.62 1.15 1.46

% Nominal conc. 100.0 99.00 96.33 102.5 98.58 98.54 103.5 100.0 100.5

Figure 4.13 Representative calibration curve of GBP

1 2 ... 61 62 63 64 65 66 67 68 69 70 71 ... 92 93

Komentáře k této Příručce

Žádné komentáře

Samsung RT34M Uživatelský manuál Strana 66

Komentáře k této Příručce

Související produkty a manuály pro ne Samsung RT34M